|
|
|
Facilities Equipment in the lab includes:
TA instruments Q500 thermogravimetric analyzer with dual mass flow controllers and evolved gas analysis furnace
Micromeritics ASAP 2010 surface area and porosity analyzer with micropore capacity. Plumbed with N2, CO2, and He.
Shimadzu 3600 UV-visible-NIR (180 nm to 3300 nm) spectrophotometer with constant-temperature stirrer liquid cell holder for in situ liquid-phase reactions.
Harrick Praying Mantis diffuse reflection holder and reaction cell with temperature control to 400°C and gas distribution manifold. Currently plumbed with He, H2/inert, O2, CO2, and a bubbler for vapor introduction.
Cart-mounted Pfeiffer Thermostar process mass spectrometer for rapid identification of desorbed species during temperature-programmed reaction (oxidation, reduction, desorption) in TGA, UV-visible-NIR spectroscopy, or standalone reactors.
JKem, IKA and home-built controlled-temperature, low pressure parallel batch reactors.
300 mL Parr autoclave reactor (3000 psi) for batch solid/liquid reactions.
190 mL Andrews glass reactor (225 psi) for batch solid/liquid reactions.
HP 6890 GC/MS and Shimadzu 2010 GC with robotic sample injector and sample tray.
Photos and user's guides will go up soon.
|
